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Oral presentation

Simultaneous determination of acidity and U(IV), U(VI) in nitrate solutions by in-line spectrophotometric technique

Suzuki, Yutaka; Nemoto, Hirokazu*; Igarashi, Kazuto*; Okano, Masanori; Kuno, Takehiko; Yamada, Keiji; Watahiki, Masaru

no journal, , 

no abstracts in English

Oral presentation

Applicability of capillary electrophoresis with pre-capillary complexation technique for analysis of uranium in radioactive wastes

Haraga, Tomoko; Kameo, Yutaka; Katayama, Atsushi; Nakashima, Mikio; Takahashi, Kuniaki; Hoshino, Hitoshi*

no journal, , 

no abstracts in English

Oral presentation

Determination of trace amounts of uranium by on-line stripping voltammetry

Taguchi, Shigeo; Namekawa, Jun*; Surugaya, Naoki; Kurosawa, Akira

no journal, , 

no abstracts in English

Oral presentation

Surface characterization of $$beta$$-FeSi$$_{2}$$ single crystal by synchrotron-radiation X-ray photoelectron spectroscopy and X-ray absorption spectroscopy

Esaka, Fumitaka; Yamamoto, Hiroyuki; Udono, Haruhiko*; Matsubayashi, Nobuyuki*; Yamaguchi, Kenji; Shamoto, Shinichi; Magara, Masaaki; Kimura, Takaumi

no journal, , 

Surface characterization of $$beta$$-FeSi$$_{2}$$ single crystal has been performed by synchrotron-radiation X-ray photoelectron spectroscopy and X-ray absorption spectroscopy.

Oral presentation

Analysis of $$^{59}$$Ni and $$^{63}$$Ni in radioactive wastes arising from nuclear research facilities

Kameo, Yutaka; Katayama, Atsushi; Haraga, Tomoko; Nakashima, Mikio; Takahashi, Kuniaki

no journal, , 

no abstracts in English

Oral presentation

Analysis of $$^{14}$$C and $$^{36}$$Cl in radioactive wastes arising from nuclear research facilities

Ishimori, Kenichiro; Kameo, Yutaka; Katayama, Atsushi; Nakashima, Mikio; Takahashi, Kuniaki

no journal, , 

no abstracts in English

Oral presentation

Analysis of alpha nuclides contained in metal waste of which surface is contaminated with radionuclides using extraction chromatography

Shimada, Asako; Haraga, Tomoko; Kameo, Yutaka; Nakashima, Mikio; Takahashi, Kuniaki

no journal, , 

As a rapid and simple analytical method for alpha nuclides in metal waste of which surface was contaminated by radionuclides, extraction chromatography using TRU resin for analysis of Pu and Am and UTEVA resin for analysis of Th and U is evaluated. The metal waste contained lots of Fe. Trivalent iron interfere the adsorption of trivalent actinides on TRU resin. Therefore, trivalent iron was reduced bivalent with excess amount of ascorbic acid. Since F$$^{-}$$ interfere the adsorption of Th on UTEVA resin, Al$$^{3+}$$ was generally added into the sample solution to mask F$$^{-}$$. Since Fe$$^{3+}$$ also can mask F$$^{-}$$, addition of Al$$^{3+}$$ was deleted. The developed schemes were examined with dissolved solution of stainless steel and good recovery of Th, U, Pu, and Am was obtained. Therefore, contaminated metal waste was analyzed using the scheme.

Oral presentation

Isotope ratio analysis of individual U and Pu particles with ICP-MS

Esaka, Fumitaka; Magara, Masaaki; Suzuki, Daisuke; Lee, C. G.; Miyamoto, Yutaka; Shinohara, Nobuo; Kimura, Takaumi

no journal, , 

Particle analysis techniques have an important role to detect undeclared nuclear activities in nuclear safeguards. With regard to the analysis of uranium particles, we have developed SIMS and FT-TIMS methods so far. The analysis of Pu particles is also necessary in near future. In this presentation, an analytical technique using ICP-MS for individual Pu particles is presented.

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